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Standard [CURRENT]

DIN 38407-37:2013-11

German standard methods for the examination of water, waste water and sludge - Jointly determinable substances (group F) - Part 37: Determination of organochlorine pesticides, polychlorinated biphenyls and chlorobenzene in water - Method using gas chromatography and mass spectrometric detection (GC-MS) after liquid-liquid extraction (F 37)

German title
Deutsche Einheitsverfahren zur Wasser-, Abwasser- und Schlammuntersuchung - Gemeinsam erfassbare Stoffgruppen (Gruppe F) - Teil 37: Bestimmung von Organochlorpestiziden, Polychlorbiphenylen und Chlorbenzolen in Wasser - Verfahren mittels Gaschromatographie und massenspektrometrischer Detektion (GC-MS) nach Flüssig-Flüssig-Extraktion (F 37)
Publication date
2013-11
Original language
German
Pages
45
Note
The publisher recommends this document in lieu of the withdrawn document DIN 38407-2:1993-02 , for which no replacement is available.

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Publication date
2013-11
Original language
German
Pages
45
Note
The publisher recommends this document in lieu of the withdrawn document DIN 38407-2:1993-02 , for which no replacement is available.
DOI
https://dx.doi.org/10.31030/2058646

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Overview

In the new Verordnung zum Schutz der Oberflächengewässer (Oberflächengewässerverordnung) (Ordinance on the protection of surface waters (Surface Waters Ordinance)) for implementation of in particular Directive 200/60/EC Wasserrahmenrichtlinie (Water Framework Directive) and 2008/105/EC Umweltqualitätsnormen (Environmental Quality Standards Directive), Annex 5 contains a list of liquid-specific pollutants for assessment of the ecological condition and ecological potential and Annex 7, Tables 1 and 2, include other pollutants for assessment of the chemical condition of surface waters. This document specifies a method for determination of selected organochlorine pesticides, polychlorinated biphenyls and chlorobenzene in water after liquid-liquid extraction and using gas chromatography and mass spectrometric detection. The method is applicable to potable, ground, surface and wastewater in mass concentrations usually from 0,005 µg/l. The amount of suspended substances in the sample should not exceed 0,05 µg/l. The limits of quantification are significantly higher for some substances, for example alpha- and beta endosulfan. The applicability of the method to other substances which are not indicated in Table 1 or other types of water is not excluded, it shall be checked on a case-to-case basis, however. This document has been prepared by NA 119-01-03-02-17 AK "SHKW mit GC/MS" ("Low-volatile hydrocarbons with GC/MS") of NA 119-01-03 AA "Wasseruntersuchung" ("Water examination") at the Water Practice Standards Committee (NAW) and has been funded by the Länderfinanzierungsprogramm "Wasser, Boden und Abfall" (federal funding programme "Water, soil and waste").

Content
ICS
13.060.50
DOI
https://dx.doi.org/10.31030/2058646

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